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<front>
<journal-meta>
<journal-id journal-id-type="publisher-id">Front. Phys.</journal-id>
<journal-title>Frontiers in Physics</journal-title>
<abbrev-journal-title abbrev-type="pubmed">Front. Phys.</abbrev-journal-title>
<issn pub-type="epub">2296-424X</issn>
<publisher>
<publisher-name>Frontiers Media S.A.</publisher-name>
</publisher>
</journal-meta>
<article-meta>
<article-id pub-id-type="publisher-id">849237</article-id>
<article-id pub-id-type="doi">10.3389/fphy.2022.849237</article-id>
<article-categories>
<subj-group subj-group-type="heading">
<subject>Physics</subject>
<subj-group>
<subject>Review</subject>
</subj-group>
</subj-group>
</article-categories>
<title-group>
<article-title>Sub-10 ps Minimum Ionizing Particle Detection With Geiger-Mode APDs</article-title>
<alt-title alt-title-type="left-running-head">Gramuglia et al.</alt-title>
<alt-title alt-title-type="right-running-head">MIPs Detection With Geiger-Mode APDs</alt-title>
</title-group>
<contrib-group>
<contrib contrib-type="author" corresp="yes">
<name>
<surname>Gramuglia</surname>
<given-names>Francesco</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
<xref ref-type="fn" rid="fn1">
<sup>&#x2020;</sup>
</xref>
<xref ref-type="corresp" rid="c001">&#x2a;</xref>
<uri xlink:href="https://loop.frontiersin.org/people/1663343/overview"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Ripiccini</surname>
<given-names>Emanuele</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
<xref ref-type="fn" rid="fn1">
<sup>&#x2020;</sup>
</xref>
<uri xlink:href="https://loop.frontiersin.org/people/1622713/overview"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Fenoglio</surname>
<given-names>Carlo Alberto</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Wu</surname>
<given-names>Ming-Lo</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Paolozzi</surname>
<given-names>Lorenzo</given-names>
</name>
<xref ref-type="aff" rid="aff2">
<sup>2</sup>
</xref>
<xref ref-type="aff" rid="aff3">
<sup>3</sup>
</xref>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Bruschini</surname>
<given-names>Claudio</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
<xref ref-type="fn" rid="fn2">
<sup>&#x2021;</sup>
</xref>
</contrib>
<contrib contrib-type="author">
<name>
<surname>Charbon</surname>
<given-names>Edoardo</given-names>
</name>
<xref ref-type="aff" rid="aff1">
<sup>1</sup>
</xref>
<xref ref-type="fn" rid="fn2">
<sup>&#x2021;</sup>
</xref>
<uri xlink:href="https://loop.frontiersin.org/people/1103929/overview"/>
</contrib>
</contrib-group>
<aff id="aff1">
<sup>1</sup>
<institution>Advanced Quantum Architecture Laboratory</institution>, <institution>Ecole Polytechnique F&#xe9;d&#xe9;rale de Lausanne (EPFL)</institution>, <addr-line>Neuchatel</addr-line>, <country>Switzerland</country>
</aff>
<aff id="aff2">
<sup>2</sup>
<institution>Departement de Physique Nucl&#xe9;aire et Corpusculaire</institution>, <institution>Universit&#xe9; de Gen&#xe8;ve</institution>, <addr-line>Geneva</addr-line>, <country>Switzerland</country>
</aff>
<aff id="aff3">
<sup>3</sup>
<institution>European Organization for Nuclear Research</institution>, <institution>CERN</institution>, <addr-line>Meyrin</addr-line>, <country>Switzerland</country>
</aff>
<author-notes>
<fn fn-type="edited-by">
<p>
<bold>Edited by:</bold> <ext-link ext-link-type="uri" xlink:href="https://loop.frontiersin.org/people/869282/overview">Mariana Frank</ext-link>, Concordia University, Canada</p>
</fn>
<fn fn-type="edited-by">
<p>
<bold>Reviewed by:</bold> <ext-link ext-link-type="uri" xlink:href="https://loop.frontiersin.org/people/694575/overview">Lucio Pancheri</ext-link>, University of Trento, Italy</p>
<p>
<ext-link ext-link-type="uri" xlink:href="https://loop.frontiersin.org/people/692326/overview">Gabriele Giacomini</ext-link>, Brookhaven National Laboratory (DOE), United States</p>
</fn>
<corresp id="c001">&#x2a;Correspondence: Francesco Gramuglia, <email>Francesco.gramuglia@epfl.ch</email>
</corresp>
<fn fn-type="equal" id="fn1">
<label>
<sup>&#x2020;</sup>
</label>
<p>These authors share the first authorship</p>
</fn>
<fn fn-type="equal" id="fn2">
<label>
<sup>&#x2021;</sup>
</label>
<p>These authors share the last authorship</p>
</fn>
<fn fn-type="other">
<p>This article was submitted to High-Energy and Astroparticle Physics, a section of the journal Frontiers in Physics</p>
</fn>
</author-notes>
<pub-date pub-type="epub">
<day>11</day>
<month>05</month>
<year>2022</year>
</pub-date>
<pub-date pub-type="collection">
<year>2022</year>
</pub-date>
<volume>10</volume>
<elocation-id>849237</elocation-id>
<history>
<date date-type="received">
<day>05</day>
<month>01</month>
<year>2022</year>
</date>
<date date-type="accepted">
<day>08</day>
<month>04</month>
<year>2022</year>
</date>
</history>
<permissions>
<copyright-statement>Copyright &#xa9; 2022 Gramuglia, Ripiccini, Fenoglio, Wu, Paolozzi, Bruschini and Charbon.</copyright-statement>
<copyright-year>2022</copyright-year>
<copyright-holder>Gramuglia, Ripiccini, Fenoglio, Wu, Paolozzi, Bruschini and Charbon</copyright-holder>
<license xlink:href="http://creativecommons.org/licenses/by/4.0/">
<p>This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.</p>
</license>
</permissions>
<abstract>
<p>Major advances in silicon pixel detectors, with outstanding timing performance, have recently attracted significant attention in the community. In this work we present and discuss the use of state-of-the-art Geiger-mode APDs, also known as single-photon avalanche diodes (SPADs), for the detection of minimum ionizing particles (MIPs) with best-in-class timing resolution. The SPADs were implemented in standard CMOS technology and integrated with on-chip quenching and recharge circuitry. Two devices in coincidence allowed to measure the time-of-flight of 180 GeV/c momentum pions with a coincidence time resolution of 22 ps FWHM (9.4 ps Gaussian sigma). Radiation hardness measurements, also presented here, highlight the suitability of this family of devices for a wide range of high energy physics (HEP) applications.</p>
</abstract>
<kwd-group>
<kwd>avalanche photodiode</kwd>
<kwd>beamline</kwd>
<kwd>particles</kwd>
<kwd>sensor</kwd>
<kwd>time-of-flight</kwd>
</kwd-group>
</article-meta>
</front>
<body>
<sec id="s1">
<title>1 Introduction</title>
<sec id="s1-1">
<title>1.1 High Timing Resolution With Silicon Pixel Detectors</title>
<p>Silicon pixel detectors have been developed in high-energy physics applications to provide precise position measurements thanks to their compactness and high spatial granularity. Recent developments have been focused on sub-100&#xa0;ps timing measurements of optical photons and direct detection of charged particles.</p>
<p>When a particle passes through the detector, electron-hole pairs are generated. When these charges move in the depletion region, an induced current pulse is registered on one electrode. According to the Schockley-Ramo theorem [<xref ref-type="bibr" rid="B1">1</xref>, <xref ref-type="bibr" rid="B2">2</xref>], this current is proportional to the free charge <italic>Q</italic>, to the speed of the charge carriers <italic>v</italic>, and to the weighting field, which can be expressed, to a first approximation, as <inline-formula id="inf1">
<mml:math id="m1">
<mml:mfrac>
<mml:mrow>
<mml:mn>1</mml:mn>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
</mml:mrow>
</mml:mfrac>
</mml:math>
</inline-formula>, where <italic>d</italic> is the thickness of the depletion region. Hence, we can calculate the induced current as:<disp-formula id="e1">
<mml:math id="m2">
<mml:mi>i</mml:mi>
<mml:mo>&#x3d;</mml:mo>
<mml:mi>k</mml:mi>
<mml:mi>Q</mml:mi>
<mml:mi>v</mml:mi>
<mml:mfrac>
<mml:mrow>
<mml:mn>1</mml:mn>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
</mml:mrow>
</mml:mfrac>
<mml:mo>,</mml:mo>
</mml:math>
<label>(1)</label>
</disp-formula>where <italic>k</italic> is a proportionality factor. The signal ends when all charges have been collected. Moreover, in case of a minimum ionizing particle (MIP) crossing a thin device, the charge <italic>Q</italic> is proportional to <italic>d</italic>. We thus have:<disp-formula id="e2">
<mml:math id="m3">
<mml:mi>i</mml:mi>
<mml:mo>&#x3d;</mml:mo>
<mml:mi>k</mml:mi>
<mml:mi>N</mml:mi>
<mml:mi>d</mml:mi>
<mml:mi>v</mml:mi>
<mml:mfrac>
<mml:mrow>
<mml:mn>1</mml:mn>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
</mml:mrow>
</mml:mfrac>
<mml:mo>&#x3d;</mml:mo>
<mml:mi>k</mml:mi>
<mml:mi>N</mml:mi>
<mml:mi>v</mml:mi>
<mml:mo>,</mml:mo>
</mml:math>
<label>(2)</label>
</disp-formula>where <italic>N</italic> is the number of electron-hole pairs generated per unit length. This result shows that the initial value of the induced current is constant and does not depend on the thickness of the depletion region. When reading out this current signal on a load, behaving like an ideal transimpedance amplifier, we observe a sharp voltage pulse. The time-of-arrival of the charge is usually determined by comparing the voltage pulse with a threshold. The uncertainty of the voltage pulse <italic>&#x3c3;</italic>
<sub>
<italic>V</italic>
</sub> is expressed as:<disp-formula id="e3">
<mml:math id="m4">
<mml:msub>
<mml:mrow>
<mml:mi>&#x3c3;</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>V</mml:mi>
</mml:mrow>
</mml:msub>
<mml:mo>&#x3d;</mml:mo>
<mml:msub>
<mml:mrow>
<mml:mi>&#x3c3;</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>t</mml:mi>
</mml:mrow>
</mml:msub>
<mml:mfrac>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>V</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>t</mml:mi>
</mml:mrow>
</mml:mfrac>
<mml:mo>,</mml:mo>
</mml:math>
<label>(3)</label>
</disp-formula>where <italic>&#x3c3;</italic>
<sub>
<italic>t</italic>
</sub> is the timing jitter of the voltage pulse. By inverting <xref ref-type="disp-formula" rid="e3">Eq. 3</xref>, we find that:<disp-formula id="e4">
<mml:math id="m5">
<mml:msub>
<mml:mrow>
<mml:mi>&#x3c3;</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>t</mml:mi>
</mml:mrow>
</mml:msub>
<mml:mo>&#x3d;</mml:mo>
<mml:mfrac>
<mml:mrow>
<mml:msub>
<mml:mrow>
<mml:mi>&#x3c3;</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>V</mml:mi>
</mml:mrow>
</mml:msub>
</mml:mrow>
<mml:mrow>
<mml:mfrac>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>V</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>t</mml:mi>
</mml:mrow>
</mml:mfrac>
</mml:mrow>
</mml:mfrac>
<mml:mo>.</mml:mo>
</mml:math>
<label>(4)</label>
</disp-formula>
</p>
<p>
<xref ref-type="disp-formula" rid="e4">Equation 4</xref> shows that the signal fluctuation (<italic>&#x3c3;</italic>
<sub>
<italic>V</italic>
</sub>) should be reduced to achieve a better timing jitter <italic>&#x3c3;</italic>
<sub>
<italic>t</italic>
</sub> and the slew rate <inline-formula id="inf2">
<mml:math id="m6">
<mml:mfrac>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>V</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
<mml:mi>t</mml:mi>
</mml:mrow>
</mml:mfrac>
</mml:math>
</inline-formula> should be maximized. In case of a sensor with an internal finite gain <italic>G</italic> [<xref ref-type="bibr" rid="B3">3</xref>&#x2013;<xref ref-type="bibr" rid="B5">5</xref>], the slew rate is proportional to <inline-formula id="inf3">
<mml:math id="m7">
<mml:mfrac>
<mml:mrow>
<mml:mi>G</mml:mi>
</mml:mrow>
<mml:mrow>
<mml:mi>d</mml:mi>
</mml:mrow>
</mml:mfrac>
</mml:math>
</inline-formula>. This analysis, where low gain avalanche diode (LGAD) concept is introduced, suggests that thin sensors with large internal gain will, in principle, result in a better timing jitter. As the LGAD signal needs amplification, the detector capacitance becomes crucial for the timing jitter. As reported in [<xref ref-type="bibr" rid="B6">6</xref>], a timing resolution of 16&#xa0;ps has been achieved with a 45&#xa0;<italic>&#x3bc;m</italic> thick and 1.7&#xa0;mm<sup>2</sup> area LGAD. There is, however, another effect that can significantly affect the pulse shape while detecting MIPs: the charge collection noise. This phenomenon is caused by the variability of the profile of the deposited charge. As shown in [<xref ref-type="bibr" rid="B7">7</xref>], this effect introduces a timing jitter that is non-negligible at the 10&#xa0;ps scale, and which increases with the detector thickness [<xref ref-type="bibr" rid="B8">8</xref>]. Various solutions have been proposed to reduce the contribution of this additional source of timing jitter, such as the detectors reported in [<xref ref-type="bibr" rid="B5">5</xref>, <xref ref-type="bibr" rid="B9">9</xref>, <xref ref-type="bibr" rid="B10">10</xref>].</p>
<p>All the effects mentioned above call for extremely high intrinsic gain and slew rate together with thin structures. Thus, Geiger-mode silicon APDs (i.e., devices biased above breakdown), also known as single-photon avalanche diodes (SPADs), could represent promising candidates for substantial timing jitter reduction [<xref ref-type="bibr" rid="B11">11</xref>]. In SPADs, unlike APDs, the avalanche is a self-sustaining process, and the timing jitter contributions are more related to the avalanche growth dynamics. In particular, the timing jitter improves, decreasing the avalanche current value needed by the frontend electronics to detect a pulse [<xref ref-type="bibr" rid="B12">12</xref>]. A comprehensive theoretical study of timing performance in SPADs when used in MIP detection is presented in [<xref ref-type="bibr" rid="B13">13</xref>]. First examples of such systems, detailed in [<xref ref-type="bibr" rid="B14">14</xref>&#x2013;<xref ref-type="bibr" rid="B16">16</xref>], were following the concept proposed by [<xref ref-type="bibr" rid="B17">17</xref>].</p>
<p>Although these potential advantages are promising, some problems usually affect Geiger-mode devices in the framework of MIP detection. Indeed, typical SPADs have a long dead time if no properly designed active quenching and recharge techniques are used [<xref ref-type="bibr" rid="B18">18</xref>]. Another issue is the presence of noise in the form of spurious pulses even in the dark. This noise, known as dark count rate (DCR), could limit the suitability of SPADs for the target application because of significant degradation of the measurement signal-to-noise ratio (SNR). However, as shown by [<xref ref-type="bibr" rid="B19">19</xref>, <xref ref-type="bibr" rid="B20">20</xref>], DCR can be drastically reduced by detecting MIPs with two SPADs operated in coincidence. Building on these elements, we present MIP time-of-flight (ToF) measurements resulting in unprecedented timing precision.</p>
</sec>
<sec id="s1-2">
<title>1.2 Single-Photon Avalanche Diodes Detector and System-On-Board</title>
<p>The detector system used in this work relies on the SPAD-based sensor presented in [<xref ref-type="bibr" rid="B21">21</xref>]. This device&#x2019;s cross-section is based on a substrate-isolated type, where a <italic>p-well</italic> (<italic>PW</italic>) layer forms the anode of the SPAD and a <italic>buried n-well</italic> (<italic>BNW</italic>) layer creates the cathode contact. The latter is connected to the high voltage through a <italic>deep-n-well</italic> (<italic>DNW</italic>). The SPAD presents a <italic>p-i-n</italic> structure [<xref ref-type="bibr" rid="B21">21</xref>]. <xref ref-type="fig" rid="F1">Figure 1A</xref> shows the cross-section of the SPAD, while <xref ref-type="fig" rid="F1">Figure 1B</xref> shows a micrograph of the sensor used in this study. The guard ring has a virtual design and employs a low doping <italic>p-Epi</italic> region located between the <italic>PW</italic> and the <italic>DNW</italic> contact to smooth the doping transition and lower the electric field. Thus, a <italic>p-Epi</italic> layer between anode and cathode allows a relatively extended and uniform high-field region (<xref ref-type="fig" rid="F2">Figure 2A</xref>).</p>
<fig id="F1" position="float">
<label>FIGURE 1</label>
<caption>
<p>
<bold>(A)</bold>: SPAD cross section. <bold>(B)</bold>: Micrograph of the implemented chip embedding 25&#xa0;<italic>&#x3bc;m</italic> diameter SPADs with integrated pixel circuit [<xref ref-type="bibr" rid="B21">21</xref>].</p>
</caption>
<graphic xlink:href="fphy-10-849237-g001.tif"/>
</fig>
<fig id="F2" position="float">
<label>FIGURE 2</label>
<caption>
<p>TCAD simulation of the 2D electric field distribution in the cross section <bold>(A)</bold>. A quantification of the electric field along the vertical axis is also shown <bold>(B)</bold> [<xref ref-type="bibr" rid="B21">21</xref>].</p>
</caption>
<graphic xlink:href="fphy-10-849237-g002.tif"/>
</fig>
<p>The sensor integrates four independent SPAD pixels with a diameter of 25&#xa0;<italic>&#x3bc;</italic>m. A dedicated on-chip front-end circuitry, shown in <xref ref-type="fig" rid="F3">Figure 3</xref>, is implemented in close proximity to each SPAD. In the SPAD front-end circuit (see <xref ref-type="fig" rid="F3">Figure 3</xref>) the cascode transistor <italic>M</italic>
<sub>1</sub> is used as a resistive divider and voltage clamp, along with <italic>M</italic>
<sub>2</sub> to enable high excess bias. This comes in combination with thin-oxide MOS transistors in the remainder of the front-end to improve the timing performance. <italic>M</italic>
<sub>2</sub> and <italic>M</italic>
<sub>3</sub> form the active recharge branch, turned on by the feedback loop composed by the NOR gate, Schmitt trigger, and tunable delay element (see <xref ref-type="fig" rid="F3">Figure 3</xref> <italic>right</italic>). The circuit is designed to enable a tunable dead time, as short as 3&#xa0;ns, supporting very high count rates while still maintaining very low afterpulsing [<xref ref-type="bibr" rid="B21">21</xref>]. Concerning the leakage current for this detector, as reported in [<xref ref-type="bibr" rid="B21">21</xref>], the measured value is on the order of 0.1&#x2013;1&#xa0;pA, which corresponds to a value of about 0.4-4&#xa0;fA/<italic>&#x3bc;m</italic>
<sup>2</sup>.</p>
<fig id="F3" position="float">
<label>FIGURE 3</label>
<caption>
<p>Device schematic. The chip output is connected to an external fast SiGe comparator to drive a 50&#xa0;&#x3a9; differential output line.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g003.tif"/>
</fig>
<p>In this work, we implemented a complete and optimized system-on-board to further improve performance. The resulting system comprises a motherboard, where all needed voltage levels are derived from a single 5&#xa0;V power supply. A power management unit was designed to filter most of the electronic noise and to provide low-noise and stable voltage levels to the detector and its front-end circuits. Moreover, the full integration of a system-on-board reduces the noise picked up in cables and power cords that can act as antennas. Indeed, reducing the noise in the system is essential when the target timing precision approaches 10&#xa0;ps [<xref ref-type="bibr" rid="B3">3</xref>]. A full system control is achieved with a serial bus interface that allows the tuning of the device operating point from an host computer.</p>
<p>The output of the chip is connected to fast SiGe comparators (Analog Device ADCMP572) that drive 50&#xa0;&#x3a9; lines (<xref ref-type="fig" rid="F3">Figure 3</xref>). This solution reduces the capacitive load at the chip&#x2019;s output (high impedance node) and helps propagate the signal through a high-frequency cable to the timestamping electronics. In addition, the use of these comparators makes it possible to achieve high signal slew rate (&#x2265;1.6&#xa0;V/ns).</p>
</sec>
</sec>
<sec id="s2">
<title>2 Optical Device Characterization</title>
<p>In order to analyze the performance of our system, we started from an optical characterization using the setup in <xref ref-type="fig" rid="F4">Figure 4</xref> [<xref ref-type="bibr" rid="B21">21</xref>, <xref ref-type="bibr" rid="B22">22</xref>]. The test bench is composed of a femtosecond pulsed laser used as the controlled light source, making the pulse length contribution to the measured timing jitter negligible. The laser beam is split into two branches. One branch is captured by a fast photodiode used as an optical, rather than electrical, reference to ensure that the dominant jitter is that of the device under test (DUT). The other branch passes through a second harmonic generation (SHG) stage to generate a light pulse in the visible range (i.e., within our device sensitivity spectrum). The latter is then attenuated, employing a neutral density filter (NDF) to reach a single-photon regime, and sent to the DUT. Finally, the output signals of the photodiode and the DUT are connected to an oscilloscope to build a time-difference histogram, representing the instrument response function (IRF). An asymmetric curve characterizes the typical SPAD IRF with the main peak, generally modeled with a Gaussian profile and an exponential tail [<xref ref-type="bibr" rid="B23">23</xref>&#x2013;<xref ref-type="bibr" rid="B25">25</xref>].</p>
<fig id="F4" position="float">
<label>FIGURE 4</label>
<caption>
<p>Experimental setup for device characterization using femtosecond pulsed lasers.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g004.tif"/>
</fig>
<p>The experiment has been repeated for several excess bias voltages and two wavelengths, and the results are shown in <xref ref-type="fig" rid="F5">Figure 5</xref>. The timing results are expressed as FWHM of the IRF. The timing precision shows a dependency on the bias point, and it improves when increasing the applied voltage, as expected. With this improved system, we reached a timing jitter of 7.5 ps at a reverse bias voltage of 28&#xa0;V, corresponding to an excess bias (<italic>V</italic>
<sub>
<italic>ex</italic>
</sub>) of about 6.5&#xa0;V. Moreover, we report in <xref ref-type="fig" rid="F5">Figure 5B</xref> the decay time constant of the exponential tail again as a function of reverse bias voltage. These results show an improvement of almost 40% with respect to what reported in [<xref ref-type="bibr" rid="B21">21</xref>], where the output was directly taken from the packaged die with high impedance 4&#xa0;GHz active probes. This optical characterization provides us with an estimation of the system performance when detecting a MIP. Indeed, the mean free path of a MIP in silicon is on the order of hundreds of nanometers. Therefore, considering the thin structure of the proposed SPADs, we expect the generation of a small amount of primary charge inside the device sensitive volume. Moreover, Geiger-mode operation and a prompt avalanche detection ensure that the output signal is the same when detecting single photons or MIPs.</p>
<fig id="F5" position="float">
<label>FIGURE 5</label>
<caption>
<p>
<bold>(A)</bold> FWHM single-photon timing resolution obtained with the designed system. <bold>(B)</bold> Exponential tail time constant measured at various excess bias voltages. For these experiments two wavelengths were used: 515 and 780&#xa0;nm. The results show a timing jitter of &#x223c;7.5&#xa0;ps FWHM for green and &#x223c;8.5&#xa0;ps FWHM for red light at &#x223c;6.5&#xa0;V of excess bias voltage.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g005.tif"/>
</fig>
</sec>
<sec id="s3">
<title>3 Time-Of-Flight Measurements for Minimum Ionizing Particles</title>
<p>The setup used for the ToF measurement of MIPs is shown in <xref ref-type="fig" rid="F6">Figure 6</xref>. It consists of two systems-on-board (see <xref ref-type="sec" rid="s1-2">Section 1.2</xref>), both mounted on motorized linear stages with sub-micrometer positioning resolution to allow a proper detector alignment and to guarantee the acquisition of coincidence measurements. We installed the setup on the H8 beamline in the CERN North Area. This beamline delivers 180&#xa0;GeV/c momentum pions produced on a graphite target by the interaction of protons accelerated by the Super Proton Synchrotron (SPS).</p>
<fig id="F6" position="float">
<label>FIGURE 6</label>
<caption>
<p>Experimental MIP coincidence measurement setup.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g006.tif"/>
</fig>
<p>The beam profile measurement is reported in <xref ref-type="fig" rid="F7">Figure 7</xref>. A good alignment between the two detectors has been achieved thanks to an HVCMOS telescope [<xref ref-type="bibr" rid="B26">26</xref>]. The two detectors were positioned at the center of the beam, where the intensity is the highest. Coincidence events were acquired for two bias voltages, 24 and 27&#xa0;V, corresponding to approximately 2.5 and 5.5&#xa0;V <italic>V</italic>
<sub>
<italic>ex</italic>
</sub>, respectively. <xref ref-type="fig" rid="F8">Figure 8</xref> shows the ToF distributions for both <italic>V</italic>
<sub>
<italic>ex</italic>
</sub>. The MIP measurement results are summarized in <xref ref-type="table" rid="T1">Table 1</xref>.</p>
<fig id="F7" position="float">
<label>FIGURE 7</label>
<caption>
<p>MIP beam profile acquired with the HVCMOS telescope described in [<xref ref-type="bibr" rid="B26">26</xref>].</p>
</caption>
<graphic xlink:href="fphy-10-849237-g007.tif"/>
</fig>
<fig id="F8" position="float">
<label>FIGURE 8</label>
<caption>
<p>Normalized distribution of the MIP time-of-flight between two SPADs in coincidence. <bold>(A)</bold> at 24&#xa0;V and <bold>(B)</bold> at 27&#xa0;V bias voltage.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g008.tif"/>
</fig>
<table-wrap id="T1" position="float">
<label>TABLE 1</label>
<caption>
<p>Summary of the MIP detection measurement results. The Gaussian sigma has been obtained by dividing the FWHM by <inline-formula id="inf4">
<mml:math id="m8">
<mml:mn>2</mml:mn>
<mml:msqrt>
<mml:mrow>
<mml:mn>2</mml:mn>
<mml:mi>l</mml:mi>
<mml:mi>n</mml:mi>
<mml:mrow>
<mml:mo stretchy="false">(</mml:mo>
<mml:mrow>
<mml:mn>2</mml:mn>
</mml:mrow>
<mml:mo stretchy="false">)</mml:mo>
</mml:mrow>
</mml:mrow>
</mml:msqrt>
</mml:math>
</inline-formula>. Assuming that the response is the same for both SPADs, the <italic>&#x3c3;</italic>
<sub>
<italic>single</italic>
</sub> values have been obtained by dividing the <italic>&#x3c3;</italic> values by <inline-formula id="inf5">
<mml:math id="m9">
<mml:msqrt>
<mml:mrow>
<mml:mn>2</mml:mn>
</mml:mrow>
</mml:msqrt>
</mml:math>
</inline-formula>. The errors have been evaluated using statistical error propagation.</p>
</caption>
<table>
<thead valign="top">
<tr>
<th align="left">Bias (V)</th>
<th align="center">FWHM (ps)</th>
<th align="center">FWTM (ps)</th>
<th align="center">
<italic>&#x3c3;</italic> (ps)</th>
<th align="center">
<italic>&#x3c3;</italic>
<sub>
<italic>single</italic>
</sub> (ps)</th>
</tr>
</thead>
<tbody valign="top">
<tr>
<td align="left">24</td>
<td align="char" char="plusmn">27 &#xb1; 1</td>
<td align="char" char="plusmn">104 &#xb1; 4</td>
<td align="char" char="plusmn">11.5 &#xb1; 0.4</td>
<td align="char" char="plusmn">8.1 &#xb1; 0.3</td>
</tr>
<tr>
<td align="left">27</td>
<td align="char" char="plusmn">22 &#xb1; 2</td>
<td align="char" char="plusmn">62 &#xb1; 3</td>
<td align="char" char="plusmn">9.4 &#xb1; 0.7</td>
<td align="char" char="plusmn">6.6 &#xb1; 0.5</td>
</tr>
</tbody>
</table>
</table-wrap>
</sec>
<sec id="s4">
<title>4 Radiation Hardness</title>
<p>The radiation hardness of the SPAD detectors was characterized by using protons to induce ionizing damage and, more importantly, displacement damage, which causes structural permanent defects [<xref ref-type="bibr" rid="B27">27</xref>, <xref ref-type="bibr" rid="B28">28</xref>]. The detectors were irradiated using the Proton Irradiation Facility (PIF) at the Paul Scherrer Institute (PSI, Villigen, Switzerland). We used a 100&#xa0;MeV mono-energetic beam with a fluence of 1 &#xd7; 10<sup>8</sup> protons per second to reach a 300&#xa0;TeV/g displacement damage dose (DDD) and 9.4&#xa0;krad total ionizing dose (TID). The DCR difference was measured 2&#xa0;weeks after the exposure with the aforementioned setup. The DCR comparison before and after the exposure is reported in <xref ref-type="fig" rid="F9">Figure 9</xref>. The characterization of the radiation hardness shows that the SPAD detector can maintain its functionality under the given radiation dose. The SPADs are not saturated by the DCR induced by the radiation damage thanks to their short dead time and high count rate. Moreover, as the ToF measurement is based on coincidence, even detectors reaching a DCR value of 1 &#xd7; 10<sup>5</sup> counts per second will not affect their particle detection performance, as also shown in [<xref ref-type="bibr" rid="B19">19</xref>, <xref ref-type="bibr" rid="B20">20</xref>]. No other degradation of the device performance was observed.</p>
<fig id="F9" position="float">
<label>FIGURE 9</label>
<caption>
<p>Radiation hardness experimental results (mean values on four devices). DCR trends over various excess bias voltages are reported. The reference with no irradiation (<italic>orange</italic>) is compared with the noise level after 100&#xa0;MeV proton irradiation (<italic>yellow</italic>), and with the samples after 1&#xa0;week of 180&#xa0;GeV/c pions irradiation.</p>
</caption>
<graphic xlink:href="fphy-10-849237-g009.tif"/>
</fig>
</sec>
<sec id="s5">
<title>5 Discussion</title>
<p>In this work we showed how Geiger-mode devices (i.e., SPADs) can detect MIPs with a sub-10 ps timing precision. This result paves the way to the implementation of future high timing resolution particle trackers based on this kind of detector. Moreover, the radiation hardness of the device was explored up to a DDD of 300&#xa0;TeV/g. After exposure, DCR increased by about three orders of magnitude, which is comparable with [<xref ref-type="bibr" rid="B29">29</xref>]. Nevertheless, this increment does not affect the timing performance of the device and does not cause the saturation of its output, thanks to the short dead time of 3&#xa0;ns guaranteed by the integrated pixel circuit on-chip. In addition, while detecting charged particles on a beamline, the number of accidental coincidences due to DCR is strongly suppressed by the logic AND between the two SPADs used for the ToF measurement [<xref ref-type="bibr" rid="B19">19</xref>]. As shown in <xref ref-type="sec" rid="s1-2">Section 1.2</xref>, in the proposed SPAD, the electric field is designed in order to have a uniform profile within the entire intrinsic layer, representing the multiplication region. Moreover, the small thickness of the charge collector region significantly reduces the charge collection noise. This two device features together with an improved front-end circuit and a maximization of the signal slew-rate are crucial when targeting sub-10 ps timing resolution.</p>
<p>When analyzing <xref ref-type="fig" rid="F8">Figure 8</xref> and the results in <xref ref-type="table" rid="T1">Table 1</xref>, we notice a dependency of the performance on the applied bias voltage. In particular, we can see a lower FWTM (full width at tenth maximum) and an improvement in the FWHM for the ToF distribution when increasing the bias point from 24 to 27&#xa0;V. The higher field improves the avalanche buildup and lateral spread time dispersion [<xref ref-type="bibr" rid="B30">30</xref>&#x2013;<xref ref-type="bibr" rid="B32">32</xref>]. Moreover, a higher bias voltage enlarges the drift region and increases the electric field inside it. This effect reduces the size of the neutral region and helps minimize the statistical spread of the diffusion and transit time needed by the primary charge carriers to reach the multiplication region [<xref ref-type="bibr" rid="B11">11</xref>].</p>
<p>Both distributions show a negligible flat background coming from random dark count coincidences. This is indicative of the efficacy of the noise filtering provided by measurements in coincidence.</p>
</sec>
</body>
<back>
<sec id="s6">
<title>Author Contributions</title>
<p>FG: Chip and board design, optical measurements, beam time measurements, data analysis, paper writing ER: ToF measurement with SPADs proposal, mechanical integration, data analysis, beam time measurements, paper writing CAF:Optical measurements, beam time measurements, data analysis, paper writing M-LW: radiation hardness measurements, data analysis, paper writing LP: Operation of the HV-CMOS telescope for SPADs alignment on beam, paper reviewing EC: Supervision, funding acquisition, paper reviewing CB: Supervision, funding acquisition, paper reviewing.</p>
</sec>
<sec id="s7">
<title>Funding</title>
<p>This research was supported, in part, by the Swiss National Science Foundation under grant 200021-169465 and Sinergia CRSII5-177165.</p>
</sec>
<sec sec-type="COI-statement" id="s8">
<title>Conflict of Interest</title>
<p>The authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest.</p>
</sec>
<sec sec-type="disclaimer" id="s9">
<title>Publisher&#x2019;s Note</title>
<p>All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations, or those of the publisher, the editors and the reviewers. Any product that may be evaluated in this article, or claim that may be made by its manufacturer, is not guaranteed or endorsed by the publisher.</p>
</sec>
<ack>
<p>We would like to thank the FASER group of the DPNC of the University of Geneva, led by Iacobucci, for the help and the support during the beamtime.</p>
</ack>
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